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[0059] When condensing the second AEEA, use a reaction system in which the molar ratio of 2-chlorotriphenyl chloride resin / Fmoc-AEEA-OH / HATU / DIPEA is 1:2:2:2.4, and react for 1.5h to obtain Fmoc-AEEA-AEEA- Resin, use 20% piperidine / DMF to deprotect after synthesis, the deprotection time is: 5+15min
Hosseini, M
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